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HRID31311

反应详情

EQUATION

反应方程式

HRID 31311 的结构方程式

REACTANTS

反应物

2
结构：O=[N+]([O-])c1ccc(Oc2ccc3c(c2)CCC(c2ccccc2)O3)nc1
HCID17978512

5-Nitro-2-[(2-phenyl-3,4-dihydro-2H-1-benzopyran-6-yl)oxy]pyridine

C20H16N2O4

结构：Oc1ccc2c(c1)OCC(c1ccccc1)C2
HCID20496761

未命名化合物

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1ccc(Oc2ccc3c(c2)OCC(c2ccccc2)C3)nc1
HCID17978505

未命名化合物

PROCEDURE

实验过程

5-Nitro-2-(3-phenylchroman-7-yloxy)pyridine was prepared as described for 5-nitro-2-(2-phenylchroman-6-yloxy)pyridine in Example 1(b) using 200 mg of 3-phenylchroman-7-ol. 1H NMR (400 MHz, d6-DMSO) δ: δ: 9.05 (d, 1H, J 2.9 Hz), 8.61 (dd, 1H, J 9.1, 2.9 Hz), 7.34-7.38 (m, 4H), 7.27-7.30 (m, 1H), 7.22 (m, 2H), 6.70-6.74 (m, 2H), 4.31 (dd, 1H, J 10.4, 3.5 Hz), 4.12 (t, 1H, 10.4 Hz), 3.24 (m, 1H), 3.01-3.11 (m, 2H).