HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 17978612, compound → 2-(3-Methoxyphenyl)chroman-4,6-diol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 17978612 | HCID 17978612 | — |
| Reactant | 2-Phenylchroman-4,6-diol | HCID 17978631 | — |
| Product | 2-(3-Methoxyphenyl)chroman-4,6-diol | HCID 17978538 | — |
Reaction Steps
2-(3-Methoxyphenyl)chroman-4,6-diol was prepared as described for 2-phenylchroman-4,6-diol in Example 8(a) starting from 6-hydroxy-2-(3-methoxyphenyl)-chroman-4-one. 1H NMR (400 MHz, d6-DMSO) δ: 8.82 (s, 1H), 7.31 (t, 1H, J 15.7, 7.9 Hz), 6.99-7.02 (m, 2H), 6.88-6.90 (m, 2H), 6.59 (d, 1H, J 8.7 Hz), 6.54 (dd, 1H, J 8.7, 2.8 Hz), 5.40 (d, 1H, J 7.0 Hz), 5.08 (d, 1H, J 11.5 Hz), 4.83-4.89 (m, 1H), 3.77 (s, 3H), 2.23-2.28 (m, 1H), 1.83-1.92 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07425568B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-d7d3809a687d465a9eb7e69d6c030431 |
| Source note | uspto-grants-2008_09 |