反应详情

温度

81 °C

A stirred mixture of 2,3-bishydrazinocarbonyl-5-bromo-7-ethyl-4-hydroxyquinoline (0.40 g, 1.1 mM) in glacial acetic acid (12 mL) was heated at 81° C. for 1.5 hr. After cooling to room temperature, the reaction mixture was filtered and the collected solids washed with acetic acid and air dried to provide the title compound (0.25 g, 70%) as a light brown solid, mp>400° C.; MS(CI): 336 (M+H).

1. temperatureAfter cooling to room temperature
2. filtrationthe reaction mixture was filtered
3. washthe collected solids washed with acetic acid and air
4. customdried