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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 31633Generated: October 25, 2026

Cyclohexanone → 1,5-Dioxaspiro[5.5]undec-3-ylmethanol

https://huagongshe.com/reaction/31633

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCyclohexanoneHCID 7967—
ReactantTrimethylolmethaneHCID 78432—
Product1,5-Dioxaspiro[5.5]undec-3-ylmethanolHCID 1528669365%

Reaction Steps

The same procedure as in the step (1a) of Example 1 was repeated using 2-(hydroxymethyl)-1,3-propanediol and cyclohexanone to obtain the title compound (2.26 g, yield: 65%) as a light yellow oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07425634B2
Source datasetuspto-grants-2008_09
ORD IDord-5cb5e6131adb45fb800cd2a1b6dcb053
Source noteuspto-grants-2008_09