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HRID31638

反应详情

EQUATION

反应方程式

HRID 31638 的结构方程式

REACTANTS

反应物

2
结构：CC1(C)OCC(CCO)CO1
HCID11816011

2-(2,2-dimethyl-1,3-dioxan-5-yl)ethanol

C8H16O3

结构：COC1OCC(COc2ccnc(CS(=O)c3nc4ccccc4[nH]3)c2C)CO1.[Na]
HCID66776002

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(OCCC2COC(C)(C)OC2)ccnc1CS(=O)c1nc2ccccc2[nH]1.[Na]
HCID66775855

未命名化合物

收率 2%

PROCEDURE

实验过程

The same procedure as in the steps (6b) to (6f) of Example 6 was repeated using 2-(2,2-dimethyl-1,3-dioxan-5-yl)ethanol obtained in the step (28a) to obtain the title compound (58 mg, total yield: 2.0%) as a light yellow solid.

WORKUP

后处理

  1. customobtained in the step (28a)