HuagongsheHuagongshe Chemistry Print Report · For research reference only
(1,3-Dioxan-2-yl)methanol → (2-Methyl-1,3-dioxan-2-yl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (1,3-Dioxan-2-yl)methanol | HCID 142350 | — |
| Reactant | 1-(Benzyloxy)propan-2-one | HCID 3691284 | — |
| Product | (2-Methyl-1,3-dioxan-2-yl)methanol | HCID 59792415 | 37% |
Reaction Steps
The same procedure as in the steps (32a) and (32b) of Example 32 was repeated using 1-benzyloxy-2-propanone to obtain the title compound (1.51 g, total yield: 37%) as a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07425634B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-db1ffc014e624f15aa85215bc7e7e9eb |
| Source note | uspto-grants-2008_09 |