HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetoacetate → 2-(2,5,5-Trimethyl-1,3-dioxan-2-yl)ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetoacetate | HCID 8868 | — |
| Reactant | Neopentyl glycol | HCID 31344 | — |
| Reactant | 2-(2-Propyl-1,3-dioxan-2-yl)ethanol | HCID 59792435 | — |
| Product | 2-(2,5,5-Trimethyl-1,3-dioxan-2-yl)ethanol | HCID 23252950 | 55% |
Reaction Steps
The same procedure as in the steps (8a) and (8b) of Example 8 was repeated using ethyl acetoacetate, and 2,2-dimethyl-1,3-propanediol to obtain the title compound (7.3 g, total yield: 55%) as a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07425634B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-3eddc8993b914b09824dff92265f7283 |
| Source note | uspto-grants-2008_09 |