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HRID31646

反应详情

EQUATION

反应方程式

HRID 31646 的结构方程式

REACTANTS

反应物

2
结构：CC1(C)COC(C)(CCO)OC1
HCID23252950

2-(2,5,5-Trimethyl-1,3-dioxan-2-yl)ethan-1-ol

C9H18O3

结构：COC1OCC(COc2ccnc(CS(=O)c3nc4ccccc4[nH]3)c2C)CO1.[Na]
HCID66776002

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(OCCC2(C)OCC(C)(C)CO2)ccnc1CS(=O)c1nc2ccccc2[nH]1.[Na]
HCID66775761

未命名化合物

收率 7.2%

PROCEDURE

实验过程

The same procedure as in the steps (6b) to (6f) of Example 6 was repeated using 2-(2,5,5-trimethyl-1,3-dioxan-2-yl)ethanol obtained in the step (34a) to obtain the title compound (196 mg, total yield: 7.2%) as a light yellow solid.

WORKUP

后处理

  1. customobtained in the step (34a)