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HRID31667

反应详情

EQUATION

反应方程式

HRID 31667 的结构方程式

REACTANTS

反应物

3
结构：Cc1c[n+]([O-])c(C)c(C)c1Cl
HCID2779141

4-Chloro-2,3,5-trimethyl-1-oxo-1lambda~5~-pyridine

C8H10ClNO

结构：OCC1(CF)OCCCO1
HCID59792600

未命名化合物

结构：Cc1c(OCC2OCC(C)(C)CO2)ccnc1CS(=O)c1nc2ccccc2[nH]1.[Na]
HCID66776588

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cnc(CS(=O)c2nc3ccccc3[nH]2)c(C)c1OCC1(CF)OCCCO1.[Na]
HCID66776537

未命名化合物

收率 12%

PROCEDURE

实验过程

The same procedure as in the steps (1c) to (1g) of Example 1 was repeated using 4-chloro-2,3,5-trimethylpyridine 1-oxide and (2-(fluoromethyl)-1,3-dioxan-2-yl)methanol to obtain the title compound (331 mg, 5 steps: 12%) as a yellow solid.