HRID31696

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID59792564

未命名化合物

结构：CCC1(CCOc2ccnc(CS(=O)c3nc4ccccc4[nH]3)c2C)OCC2(CO1)OCCO2.[Na]

HCID66776196

未命名化合物

PRODUCTS

生成物

结构：Cc1c(OCCC2(C)OCC3(CO2)OCCO3)ccnc1CS(=O)c1nc2ccccc2[nH]1.[Na]

HCID66775866

未命名化合物

收率 15.1%

PROCEDURE

实验过程

The same procedure as in the steps (4f) to (4j) of Example 4 was repeated using 2-(8-methyl-1,4,7,9-tetraoxaspiro[4.5]dec-8-yl)ethanol obtained in the step (73b) above to obtain the title compound (298 mg, total 15.1% yield) as a white solid.

WORKUP

后处理

customobtained in the step (73b) above