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HRID31704

反应详情

EQUATION

反应方程式

HRID 31704 的结构方程式

REACTANTS

反应物

2
结构：OCC1CCCC12OCCO2
HCID10487146

(1,4-Dioxaspiro[4.4]nonan-6-yl)methanol

C8H14O3

结构：Cc1c(OC[C@@H]2COC(C)(C)O2)ccnc1CS(=O)c1nc2ccccc2[nH]1.[Na]
HCID66776552

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(OCC2CCCC23OCCO3)ccnc1CS(=O)c1nc2ccccc2[nH]1.[Na]
HCID66775624

未命名化合物

PROCEDURE

实验过程

The same procedure as in the steps (14a) to (14e) of Example 14 was repeated using the 1,4-dioxaspiro[4.4]non-6-ylmethanol obtained in the step (80b) above to obtain the title compound (383 mg, the total yield of 5 steps: 14.6%) as a light yellow solid. Note that in the same process as in the step (14c), methanol was used as a solvent instead of ethanol.

WORKUP

后处理

  1. customobtained in the step (80b) above