HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2,4-Dichlorophenyl)-2-morpholin-4-ylethan-1-one → HCID 69308798, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2,4-Dichlorophenyl)-2-morpholin-4-ylethan-1-one | HCID 22142875 | — |
| Solvent | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Product | HCID 69308798 | HCID 69308798 | — |
Reaction Steps
1 mmol of 1-(2,4-dichlorophenyl)-2-morpholin-4-ylethan-1-one was heated to 80° C. in N,N-dimethylformamidedimethyl acetal for six hours. The reaction mixture was concentrated in vacuo and purified by trituration with diethyl ether to obtain (2E)-1-(2,4-dichlorophenyl)-3-(dimethylamino)-2-morpholin-4-ylprop-2-en-1-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07425557B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-c687a28df77444698c82f81ab7f8d6d0 |
| Source note | uspto-grants-2008_09 |