2-Morpholinoethanol → HCID 22142773, compound

HRID 31936Notes

Reaction equation

HRID 31936 reaction equation
[CH3:1][N:2]([CH3:30])[CH2:3][CH2:4][N:5]([CH2:18][CH2:19][NH:20][C:21]1[CH:26]=[CH:25][C:24]([N+:27]([O-:29])=[O:28])=[CH:23][N:22]=1)[S:6]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[N+:15]([O-:17])=[O:16])(=[O:8])=[O:7].OCCN1C[CH2:38][O:37][CH2:36]C1>>[N:2]1([CH2:3][CH2:4][N:5]([CH2:18][CH2:19][NH:20][C:21]2[CH:26]=[CH:25][C:24]([N+:27]([O-:29])=[O:28])=[CH:23][N:22]=2)[S:6]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[N+:15]([O-:17])=[O:16])(=[O:7])=[O:8])[CH2:30][CH2:38][O:37][CH2:36][CH2:1]1

Participants

3

Reactant 2

HCID 611632-MorpholinoethanolHCID 22142494[2-(Dimethylamino) ethyl]{2-[(5-nitro(2-pyridyl))amino]ethyl}[(2-nitrophenyl)sulfonyl]amine

Product 1

HCID 22142773HCID 22142773, compound

Procedure

Made using the same procedure as for polymer-bound [2-(dimethylamino)ethyl]{2-[(5-nitro(2-pyridyl))amino]ethyl}[(2-nitrophenyl)sulfonyl]amine except that 4-(2-hydroxyethyl)morpholine (5.1 mL, 42 mmol) was used.

Sources & evidence

ORD record
ord-c35c1b2444a44bd4a73c55c53dcc2698
Source dataset
uspto-grants-2008_09
Patent number
US07425557B2

Reaction notes

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