HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-t-Butylcyclohex-1-enyl)-2-nitrobenzene → 2-(4-t-Butylcyclohexyl)phenylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-t-Butylcyclohex-1-enyl)-2-nitrobenzene | HCID 23141753 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-(4-t-Butylcyclohexyl)phenylamine | HCID 19754731 | — |
Reaction Steps
A mixture of 1-(4-t-butylcyclohex-1-enyl)-2-nitrobenzene (4.89 g, 18.86 mmol) prepared in Example (2b), 10% palladium on carbon (1.5 g, wet) and ethyl acetate (25 mL) was stirred for 4 hours under a hydrogen atmosphere at atmospheric pressure and room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07425554B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-fe3a56863eae404aba02cd4e4a3f30c5 |
| Source note | uspto-grants-2008_09 |