HuagongsheHuagongshe Chemistry Print Report · For research reference only
(+/-)trans-1-Benzoyl-3,4-diazidopiperidine → HCID 69853211, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (+/-)trans-1-Benzoyl-3,4-diazidopiperidine | HCID 86750632 | — |
| Catalyst | Lindlars catalyst | HCID 131709914 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69853211 | HCID 69853211 | — |
Reaction Steps
A solution of the diazide (D26) (450 mg, 1.7 mmol) in ethanol (30 ml) was treated with Lindlar catalyst (5% Pd/CaCO3, 250 mg) and stirred under hydrogen (1 atm) for 24 hour. The mixture was filtered and solvent removed in vacuo to afford the title compound as oil, 350 mg (94%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211107B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-446c20ba01a9409da2ada87ae8675022 |
| Source note | uspto-grants-2001_04 |