Benzyl isocyanate → HCID 15523794, compound

HRID 321945Notes

Reaction equation

[C:1]1([S:7]([CH2:9][C@@H:10]2[NH:13][C:12](=[O:14])[CH2:11]2)=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:15]([N:22]=[C:23]=[O:24])[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>>[CH2:15]([NH:22][C:23]([N:13]1[C:12](=[O:14])[CH2:11][C@@H:10]1[CH2:9][S:7]([C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1)=[O:8])=[O:24])[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

Participants

Reactant 2

HCID 76639Benzyl isocyanate

HCID 53941948HCID 53941948, compound

Product 1

HCID 15523794HCID 15523794, compound

Procedure

Following the same procedure as in example 4, step D, but using 4(R)-(benzenesulfinylmethyl)azetidin-2-one and benzylisocyanate as the starting material, gave 2(R)-benzenesulfinylmethyl-4-oxoazetidine-1-carboxylic acid benzyl amide.

Sources & evidence

ORD record: ord-fd3f12c994f143c195650a926bf4628f
Source dataset: uspto-grants-2001_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06211170B1

Reaction notes

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