Pyridine → HCID 70226372, compound

Participants

Reaction Steps

4-Methoxy-2-nitroaniline (47.6 mmole, 8.0 g) is added to a solution of pyridine (71.4 mmole, 5.8 ml) in dichloromethane (130 ml). Phenylacetyl chloride (40.6 mmole, 6.3 ml) in dichloromethane (40 ml) is slowly added, and the mixture is stirred at room temperature for two days. The mixture is washed with 10% HCl (3×), the organic layer is dried with Na2SO4, is filtered and evaporated. Recrystallisation from ethyl acetate gives the title product.

Provenance & Evidence