HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → Acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 3101369 | HCID 3101369 | — |
| Catalyst | Iron | HCID 23925 | — |
| Product | Acetate | HCID 175 | — |
| Product | 2-Benzyl-5-methoxy-1H-benzo[D]imidazole | HCID 22008503 | — |
Reaction Steps
Iron (Fe) (124.7 mmole, 6.97 g) is added to a solution of N-(4-methoxy-2-nitrophenyl) phenylacetamide (18.5 mmole, 5.0 g) in acetic acid (130 ml). The mixture is refluxed for two hours and is stirred at room temperature for 48 hours. The solvent is evaporated. Recrystallisation from ethyl. acetate gives the title product as a light yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211177B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-b577a6d1b1b64c94a0c18eb6b74e15ec |
| Source note | uspto-grants-2001_04 |