HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4-Pyridyl)aniline → 3-[3-(4-Pyridyl)Anilino]-3-Cyclobutene-1,2-Dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4-Pyridyl)aniline | HCID 459523 | — |
| Reactant | 3-Butoxycyclobut-3-ene-1,2-dione | HCID 15723182 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-[3-(4-Pyridyl)Anilino]-3-Cyclobutene-1,2-Dione | HCID 9837831 | 76.8% |
Reaction Steps
A solution of 4-(3-aminophenyl)pyridine (0.81 g) and 3-n-butoxy-3-cyclobutene-1,2-dione (0.73 g) in ethanol (20 ml) is stirred at ambient temperature for 15 hours. The resultant precipitated solid is washed with methanol and ether and recrystallized from dimethyl formamide to give 0.91 g of the title compound, mp 252-255.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211220B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-f402d218b9ee48c28e8843565ed69c3d |
| Source note | uspto-grants-2001_04 |