HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69711854, compound → HCID 69710297, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69711854 | HCID 69711854 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69710297 | HCID 69710297 | — |
Reaction Steps
A mixture of 2-8 (400 mg, 0.86 mmol) and 10% Pd/carbon (1300 mg) in EtOH (10 mL) was stirred under a balloon of hydrogen for 6 h. Following filtration and evaporative removal of the solvent, the residue was chromatographed (silica gel, 70:25:5 chloroform/ethyl acetate/MeOH) to give 2-9 as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211191B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-f18b94c4e4c542fcaf793cd034d85a27 |
| Source note | uspto-grants-2001_04 |