HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → HCID 22009638, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 22009681 | HCID 22009681 | — |
| Product | HCID 22009638 | HCID 22009638 | 97% |
Reaction Steps
In substantially the same manner as in Reference Example 12, 6-[4-[2-[(E)-2-phenylethenyl]-4-oxazolyl methoxy]phenyl]hexanol was allowed to react with methanesulfonyl chloride to give 6-[4-[2-[(E)-2-phenyl ethenyl]-4-oxazolylmethoxy]phenyl]hexyl methanesulfonate. The yield was 97%. Recrystallization from ethyl acetate-hexane gave colorless prisms, mp 88-89° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-8958eaf470c14924ae342474e0bd5488 |
| Source note | uspto-grants-2001_04 |