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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 322248Generated: October 30, 2026

Methanesulfonyl chloride → HCID 22009736, compound

https://huagongshe.com/reaction/322248

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanesulfonyl chlorideHCID 31297—
ReactantHCID 22009801HCID 22009801—
ProductHCID 22009736HCID 2200973694%

Reaction Steps

In substantially the same manner as in Reference Example 12, 3-[4-methoxy-3-[2-[(E)-2-phenylethenyl]-4-oxazolylmethoxy]phenyl]propanol was allowed to react with methanesulfonyl chloride to give 3-[4-methoxy-3-[2-[(E)-2-phenylethenyl]-4-oxazolylmethoxy]phenyl]propyl methanesulfonate. The yield was 94%. Recrystallization from ethyl acetate-hexane gave pale yellow needles, mp 112-113° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06211215B1
Source datasetuspto-grants-2001_04
ORD IDord-d5b41c6ba7a042659d81e603c5c2305e
Source noteuspto-grants-2001_04