HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dichloroacetone → HCID 11806574, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dichloroacetone | HCID 10793 | — |
| Reactant | Benzofuran-2-carboxamide | HCID 687121 | — |
| Product | HCID 11806574 | HCID 11806574 | 30% |
Reaction Steps
In substantially the same manner as in Reference Example 47, 2-benzofurancarboxamide was allowed to react with 1,3-dichloroacetone to give 2-(2-benzofuranyl)-4-chloromethyloxazole. The yield was 30%. Recrystallization from ethyl acetate-hexane gave colorless needles, mp 133-134° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-f99bc33560fb4c478d86678dbb3b3433 |
| Source note | uspto-grants-2001_04 |