Methanesulfonyl chloride → 3-(3-Benzyloxyphenyl)propyl methanesulfonate

HRID 322308Notes

Reaction equation

[CH2:1]([O:8][C:9]1[CH:10]=[C:11]([CH2:15][CH2:16][CH2:17][OH:18])[CH:12]=[CH:13][CH:14]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:19][S:20](Cl)(=[O:22])=[O:21]>>[CH3:19][S:20]([O:18][CH2:17][CH2:16][CH2:15][C:11]1[CH:12]=[CH:13][CH:14]=[C:9]([O:8][CH2:1][C:2]2[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=2)[CH:10]=1)(=[O:22])=[O:21]

Participants

Reactant 2

HCID 31297Methanesulfonyl chloride

HCID 126481553-(Phenylmethoxy)benzenepropanol

Product 1

HCID 227333633-(3-Benzyloxyphenyl)propyl methanesulfonate

Procedure

In substantially the same manner as in Reference Example 85, 3-(3-benzyloxyphenyl)propanol was allowed to react with methanesulfonyl chloride to give 3-(3-benzyloxyphenyl)propyl methanesulfonate. The yield was quantative. Oily substance.

Sources & evidence

ORD record: ord-a244c884dc0c4db2a7345d7bf81859a0
Source dataset: uspto-grants-2001_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06211215B1

Reaction notes

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