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HRID322365

反应详情

EQUATION

反应方程式

HRID 322365 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)c1nc[nH]c1C(=O)OC
HCID76810

1H-Imidazole-4,5-dicarboxylic acid, dimethyl ester

C7H8N2O4

结构：CS(=O)(=O)OCCCc1ccc(OCc2coc(/C=C/c3ccccc3)n2)cc1
HCID15521674

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)c1ncn(CCCc2ccc(OCc3coc(/C=C/c4ccccc4)n3)cc2)c1C(=O)OC
HCID22009793

未命名化合物

收率 63%

PROCEDURE

实验过程

In substantially the same manner as in Working Example 25, 3-[4-[2-[(E)-2-phenylethenyl]-4-oxazolylmethoxy]phenyl]propyl methanesulfonate was allowed to react with dimethyl 4,5-imidazoledicarboxylate to give dimethyl 1-[3-[4-[2-[(E)-2-phenylethenyl]-4-oxazolylmethoxy]phenyl]propyl]-4,5-imidazoledicarboxylate. The yield was 63%. Recrystallization from ethyl acetate-hexane gave colorless prisms, mp 85-86° C.