HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13282937, compound → HCID 22009870, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13282937 | HCID 13282937 | — |
| Reactant | 1-[3-(4-Hydroxyphenyl)propyl]imidazole | HCID 22009818 | — |
| Product | HCID 22009870 | HCID 22009870 | 66% |
Reaction Steps
In substantially the same manner as in Working Example 48, 1-[3-(4-hydroxyphenyl)propyl]imidazole was allowed to react with 4-chloromethyl-5-methyl-2-[(E)-2-phenylethenyl]oxazole to give 4-[4-[3-(1-imidazolyl)propyl)phenoxymethyl]-5-methyl-2-[(E)-2-phenylethenyl]oxazole. The yield was 66%. Recrystallization from ethyl acetate-hexane gave pale yellow prisms, mp 94-95° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-7efda4724b944844a2bbf7e67468df5a |
| Source note | uspto-grants-2001_04 |