HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22009717, compound → HCID 22009642, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22009717 | HCID 22009717 | — |
| Reactant | 1-[3-(4-Hydroxyphenyl)propyl]imidazole | HCID 22009818 | — |
| Product | HCID 22009642 | HCID 22009642 | 55% |
Reaction Steps
In substantially the same manner as in Working Example 72, 1-[3-(4-hydroxyphenyl)propyl]imidazole was allowed to react with 4-chloromethyl-2-(5-ethyl-2-thienyl)oxazole to give 2-(5-ethyl-2-thienyl)-4-[4-[3-(1-imidazolyl)propyl]phenoxymethyl]oxazole. The yield was 55%. Recrystallization from ethyl acetate-hexane gave colorless prisms, mp 57-58° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-3b762da35fd74fcab27b44245741f2bd |
| Source note | uspto-grants-2001_04 |