HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22009778, compound → HCID 22009859, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22009778 | HCID 22009778 | — |
| Reactant | 1-[3-(4-Hydroxyphenyl)propyl]imidazole | HCID 22009818 | — |
| Product | HCID 22009859 | HCID 22009859 | 53% |
Reaction Steps
In substantially the same manner as in Working Example 109, 1-[3-(4-hydroxyphenyl)propyl]imidazole was allowed to react with 5-(4-chloromethyl-2-oxazolyl)-2-phenylbenzoxazole to give 5-[4-[4-[3-(1-imidazolyl)propyl]phenoxymethyl]-2-oxazolyl]-2-phenylbenzoxazole. The yield was 53%. Recrystallization from ethyl acetate-hexane gave pale yellow prisms, mp 166-167° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211215B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-40e68439589b46cda4795a1b1d014bc6 |
| Source note | uspto-grants-2001_04 |