HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 322554Generated: November 1, 2026
Trifluoroacetic acid → D-Arg(Tos)-Gly-OBn
https://huagongshe.com/reaction/322554
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 178427593 | HCID 178427593 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | D-Arg(Tos)-Gly-OBn | HCID 178427563 | — |
Reaction Steps
A 1 g portion of Boc—(D)—Arg(Tos)—Gly—OBn (1.74 mmol) was dissolved in 10 mL of CH2Cl2, cooled to 0° C. and treated with 10 mL of TFA. The solution was stirred at 0° C. for 3 h. Solvent and excess TFA were evaporated thoroughly to give the title compound as an oil which was used directly in Example 10.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06211154B1 |
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| Source dataset | uspto-grants-2001_04 |
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| ORD ID | ord-a810cd1ced994dd0a8248ea9fcfaf747 |
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| Source note | uspto-grants-2001_04 |
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