HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → Cyanoacetyldibenzylurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Cyanoacetic acid | HCID 9740 | — |
| Reactant | Urea, N,N'-bis(phenylmethyl)- | HCID 72889 | — |
| Solvent | Water | HCID 962 | — |
| Product | Cyanoacetyldibenzylurea | HCID 20642783 | — |
Reaction Steps
36.0 g (0.15 mol) of dibenzylurea, 15.3 g (0.18 mol) of cyanoacetic acid and 30.6 g (0.3 mol) of acetic anhydride are stirred at 80-85° C. for 2 hours. After cooling, the reaction mixture is stirred into 600 ml of water and the resultant precipitate is filtered off with suction and then dried to constant weight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211270B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-c240c421fc754ef49d6d0795e73d913e |
| Source note | uspto-grants-2001_04 |