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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 322644생성일: 2026년 10월 25일

3-Pyridineacetic acid, hydrochloride (1:1) → N-[(3pyridyl)acetyl]-D,L-alanine iso-butyl ester

https://huagongshe.com/reaction/322644

반응식

참여 물질

역할이름HCID투입량
반응물3-Pyridineacetic acid, hydrochloride (1:1)HCID 2723724—
반응물2-Methylpropyl 2-aminopropanoate hydrochlorideHCID 86200109—
생성물N-[(3pyridyl)acetyl]-D,L-alanine iso-butyl esterHCID 22492127—

반응 단계

Following General Procedure F′ and using 3-pyridylacetic acid hydrochloride (Aldrich) and D,L-alanine iso-butyl ester hydrochloride (from Example B′ above), the title compound was prepared as a solid having a melting point of 62°-64° C. The reaction was monitored by tlc on silica gel (Rf=0.48 10% methanol/dichloromethane) and purification was by silica gel chromatography.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06211235B1
출처 데이터셋uspto-grants-2001_04
ORD IDord-e6860779d4444903abb55a298db6490e
출처 메모uspto-grants-2001_04