HuagongsheHuagongshe Chemistry Print Report · For research reference only
methyl (2S)-2-aminopentanoate hydrochloride → Methyl N-[N-(3-nitrophenylacetyl)-L-alaninyl]-(S)-2-aminopentanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | methyl (2S)-2-aminopentanoate hydrochloride | HCID 14118488 | — |
| Reactant | N-(3-Nitrophenylacetyl)-L-alanine | HCID 53788870 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | Methyl N-[N-(3-nitrophenylacetyl)-L-alaninyl]-(S)-2-aminopentanoate | HCID 22894966 | — |
Reaction Steps
Following General Procedure C and using N-(3-nitrophenylacetyl)-L-alanine (from Example D11 above) and methyl (S)-2-aminopentanoate hydrochloride (prepared from (S)-2-aminopentanoic acid (Novabiochem) using General Procedure H), the title compound was prepared as a solid. The reaction was monitored by tlc (Rf=0.4 in 9:1 CHCl3/MeOH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211235B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-8ba4e26444dd4ede8236510a13b4a31b |
| Source note | uspto-grants-2001_04 |