HuagongsheHuagongshe Chemistry Print Report · For research reference only
Leucine methyl ester hydrochloride → HCID 22895018, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Leucine methyl ester hydrochloride | HCID 2723695 | — |
| Reactant | N-(3-Nitrophenylacetyl)-L-alanine | HCID 53788870 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 22895018 | HCID 22895018 | — |
Reaction Steps
Following General Procedure C and using N-(3-nitrophenylacetyl)-L-alanine (from Example DI I above) and L-leucine methyl ester hydrochloride (Aldrich), the title compound was prepared as a solid. The reaction was monitored by tlc (Rf=0.75 in 9:1 CHCl3/MeOH) and the product was purified by silica gel chromatography using 97:3 CHCl3/MeOH as the eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211235B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-c5aa1efc7f244b8da4998f9bd8a6b414 |
| Source note | uspto-grants-2001_04 |