HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 322800Generated: October 30, 2026
Alpha-Methylstyrene → HCID 22011381, compound
https://huagongshe.com/reaction/322800
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Alpha-Methylstyrene | HCID 7407 | — |
| Reactant | 1-Hydroxy-4-benzoyloxy-2,2,6,6-tetramethylpiperidine | HCID 688178 | — |
| Product | HCID 22011381 | HCID 22011381 | — |
Reaction Steps
A mixture of 1.0 g (3.6 mmol) of 1-oxyl-4-benzoyloxy-2,2,6,6-tetramethylpiperidine and 10 g (85 mmol) of α-methylstyrene under a nitrogen atmosphere is heated at 120° C. for 36 hours. The reaction mixture is concentrated in vacuo and the title compound is isolated as a pale yellow oil after column chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06211378B1 |
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| Source dataset | uspto-grants-2001_04 |
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| ORD ID | ord-33bf82921bf7468e8f73dabd83e28918 |
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| Source note | uspto-grants-2001_04 |
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