HRID322813
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
To 19.6 g (0,1 mol) of 1-cyano-1-n-pentanoylaminocyclopentane dissolved in 70 ml of methanol, 5 g of Varion AD resin was added the reaction mixture was heated under reflux conditions for 3 hours. After filtration and evaporation 16.5 g (71.7%) of title compound was obtained, assay by GC: 92%.
WORKUP
后处理
- addition5 g of Varion AD resin was added the reaction mixture
- temperaturewas heated under reflux conditions for 3 hours
- filtrationAfter filtration
- customevaporation 16.5 g (71.7%) of title compound
- customwas obtained