HRID322813

反应详情

EQUATION

反应方程式

HRID 322813 的结构方程式

PROCEDURE

实验过程

To 19.6 g (0,1 mol) of 1-cyano-1-n-pentanoylaminocyclopentane dissolved in 70 ml of methanol, 5 g of Varion AD resin was added the reaction mixture was heated under reflux conditions for 3 hours. After filtration and evaporation 16.5 g (71.7%) of title compound was obtained, assay by GC: 92%.

WORKUP

后处理

  1. addition5 g of Varion AD resin was added the reaction mixture
  2. temperaturewas heated under reflux conditions for 3 hours
  3. filtrationAfter filtration
  4. customevaporation 16.5 g (71.7%) of title compound
  5. customwas obtained