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HRID32295

反应详情

EQUATION

反应方程式

HRID 32295 的结构方程式

REACTANTS

反应物

2
结构：CCOCC
HCID3283

Diethyl Ether

C4H10O

结构：C=CS(=O)(=O)C=C.CC(C)C[C@H](NC(=O)OC(C)(C)C)C(=O)O
HCID131724030

未命名化合物

PRODUCTS

生成物

1
结构：C=CS(=O)(=O)C=C.CC(C)C[C@H](N)C(=O)O.Cc1ccc(S(=O)(=O)O)cc1
HCID131724029

未命名化合物

PROCEDURE

实验过程

An Et2O solution of anhydrous p-Tosic acid (3 equiv.) was added to dry oil of Boc-Leu-vinylsulfone (1 equiv.) and stirred at room temperature overnight. The product formed a white precipitate which was recovered by centrifugation.

WORKUP

后处理

  1. customThe product formed a white precipitate which
  2. customwas recovered by centrifugation