反应详情

2,3 difluoro 6-nitro phenol (2 g, 11 mmol) was treated with 10% Pd/C (1 g) at 23° C. The reaction mixture was flushed with hydrogen gas and the reaction was allowed to stir 12 h before it was filtered through celite. The filtrate was concentrated in vacuo to afforded the title compound (1.6 g, 97%). EI-MS m/z 146 (M+H)+

1. customThe reaction mixture was flushed with hydrogen gas
2. filtrationwas filtered through celite
3. concentrationThe filtrate was concentrated in vacuo