Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 323064Generated: October 29, 2026

(1,1'-Biphenyl)-3-ol, 4-nitro- → 2-Amino-5-phenylphenol

https://huagongshe.com/reaction/323064

Reaction equation

Participants

RoleNameHCIDCharge
Reactant(1,1'-Biphenyl)-3-ol, 4-nitro-HCID 87437—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
Product2-Amino-5-phenylphenolHCID 20376—

Reaction Steps

A solution of 2-nitro 5-phenyl phenol (1.2 g, 5.5 mmol) in methanol was treated with 10% Pd/C (1.2 g). The reaction mixture was flushed with hydrogen and allowed to stir overnight. The reaction mixture was filtered through celite and the filtrate was concentrated in vacuo to afford desired (1.01 g, 98%). EI-MS m/z 186 (M+H)+

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06211373B1
Source datasetuspto-grants-2001_04
ORD IDord-c32fa1b1e52248bfb038368028e9029b
Source noteuspto-grants-2001_04