HCID 22010607, compound → HCID 22010923, compound

Participants

Reaction Steps

A solution of N-cyclopentyl-N-(4-nitrobenzoyl)-p-anisidine (1.0 g), 10% palladium on carbon (100 mg) and 2 drops of conc. hydrochloric acid in methanol (10 ml) was stirred under 3 atmospheric pressure of hydrogen at ambient temperature. After 4 hours, the reaction mixture was filtered through a bed of Celite, and concentrated to give N-(4-aminobenzoyl)-N-cyclopentyl-p-anisidine (870 mg), which was used directly for the next step without further purification.

Provenance & Evidence