HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22010808, compound → HCID 22010761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22010808 | HCID 22010808 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22010761 | HCID 22010761 | 0.1% |
Reaction Steps
A solution of 4-(4′-methylbiphenyl-2-carboxamido)-N-methyl-N-(2-allylphenyl)benzamide (100 g) and 10% palladium on carbon (20 mg) in methanol (15 ml) was stirred under an atmospheric pressure of hydrogen at ambient temperature. After 3 hours, the reaction mixture was filtered through a bed of Celite, concentrated and then triturated from diethyl ether to give 4-(4′-methylbiphenyl-2-carboxamido)-N-methyl-N-(2-propylphenyl)benzamide (70 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211242B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-1b3e1caa96cf452bb3fcea472a9ef073 |
| Source note | uspto-grants-2001_04 |