2-(Pyridin-4-yl)acetonitrile → HCID 53721703, compound

HRID 323348Notes

Reaction equation

HRID 323348 reaction equation
[N:1]1[CH:6]=[CH:5][C:4]([CH2:7][C:8]#[N:9])=[CH:3][CH:2]=1.[C:10]([O:13][CH2:14][CH3:15])(=[O:12])[CH3:11].CCCC[CH2:20][CH3:21]>>[CH2:14]([O:13][C:10](=[O:12])[CH2:11][C:7]([C:8]#[N:9])([C:4]1[CH:5]=[CH:6][N:1]=[CH:2][CH:3]=1)[CH2:11][C:10]([O:13][CH2:20][CH3:21])=[O:12])[CH3:15]

Participants

3

Reactant 2

HCID 41120852-(Pyridin-4-yl)acetonitrileHCID 21226206Ethyl acetate hexane

Product 1

HCID 53721703HCID 53721703, compound

Procedure

Prepare by the method of Example 49.1.2 using 4-pyridineacetonitrile to give, after chromatography on silica gel eluting with ethyl acetate/hexane 1/1, the title compound.

Workup

  1. customto give

Sources & evidence

ORD record
ord-29b3d2309a0b492c950478b0f73f0ba1
Source dataset
uspto-grants-2001_04
Patent number
US06211199B1

Reaction notes

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