HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 9794620, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 54474819 | HCID 54474819 | — |
| Product | HCID 9794620 | HCID 9794620 | 50.4% |
Reaction Steps
The title compound was prepared by the general procedure described in Example 1 using (cis)-2-(2,3-dihydrobenzofuran-4-yl)cycloprop-1-yl methyl amine (0.79 mmol), triethylamine (2.37 mmol) and acetyl chloride (0.95 mmol). Purification by silica gel column chromatography (Hex:EtOAc, 1:1) provided 92 mg of the desired product (50%) as an off-white wax. HPLC purity=93%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06214869B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-c68eab42cc8d44b49379ece219900930 |
| Source note | uspto-grants-2001_04 |