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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 323771Generated: October 30, 2026

Acetyl chloride → HCID 9794620, compound

https://huagongshe.com/reaction/323771

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetyl chlorideHCID 6367—
ReactantTriethylamineHCID 8471—
ReactantHCID 54474819HCID 54474819—
ProductHCID 9794620HCID 979462050.4%

Reaction Steps

The title compound was prepared by the general procedure described in Example 1 using (cis)-2-(2,3-dihydrobenzofuran-4-yl)cycloprop-1-yl methyl amine (0.79 mmol), triethylamine (2.37 mmol) and acetyl chloride (0.95 mmol). Purification by silica gel column chromatography (Hex:EtOAc, 1:1) provided 92 mg of the desired product (50%) as an off-white wax. HPLC purity=93%.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06214869B1
Source datasetuspto-grants-2001_04
ORD IDord-c68eab42cc8d44b49379ece219900930
Source noteuspto-grants-2001_04