Triethylamine → HCID 9881625, compound

Participants

Reaction Steps

The title compound was prepared by the general procedure -described in Example 1 using (cis)-2-(2,3-dihydrobenzofuran-4-yl)cycloprop-1-yl methyl amine (0.79 mmol), triethylamine (2.37 mmol) and butyryl chloride (0.95 mmol). Purification by silica gel column chromatography (Hex:EtOAc, 2:1) provided 61 mg of the desired product (30%) as a white solid. HPLC purity=98%. m.p. 73-74°;

Provenance & Evidence