HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 88219091, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | 3-(2-Amino-1-hydroxyethyl)-4-methoxybenzene-1-sulfonamide | HCID 9906041 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 88219091 | HCID 88219091 | — |
Reaction Steps
One equivalent of methanesulphonic acid in 2M solution in methanol is added to the product obtained in step 1.2. after recrystallization in methanol and diethyl ether and drying in a desiccator under vacuum over phosphorus pentoxide, 0.370 g of product is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06214882B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-f7767ae98b5f4a4bbe43bf1d4b0d3c41 |
| Source note | uspto-grants-2001_04 |