HuagongsheHuagongshe Chemistry Print Report · For research reference only
(5-Bromopentyl)benzene → 2-Acetamido-1,3-bis(tert-butyldimethylsilyloxy)-2-(2-(4-(1hydroxy-6-phenylhexyl)phenyl)ethyl)propane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (5-Bromopentyl)benzene | HCID 285561 | — |
| Reactant | 2-Acetamido-1,3-bis(tert-butyldimethylsilyloxy)-2-(2-(4-formylphenyl)ethyl)propane | HCID 15516678 | — |
| Product | 2-Acetamido-1,3-bis(tert-butyldimethylsilyloxy)-2-(2-(4-(1hydroxy-6-phenylhexyl)phenyl)ethyl)propane | HCID 22178489 | 69.2% |
Reaction Steps
2-Acetamido-1,3-bis(tert-butyldimethylsilyloxy)-2-(2-(4-formylphenyl)ethyl)propane (3.0 g) and 1-bromo-5-phenylpentane (4.1 g) were reacted and treated in the same manner as in Working example 1(6) to give the title compound (2.7 g) as a pale yellow oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06214873B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-db71ff42a718470e8a83e65d75092ced |
| Source note | uspto-grants-2001_04 |