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(6-Bromohexyl)benzene → 2-Acetamido-1,3-bis(tert-butyldimethylsilyloxy)-2-(2-(4-(1-hydroxy-7-phenylheptyl)phenyl)ethyl)propane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (6-Bromohexyl)benzene | HCID 561788 | — |
| 反応物 | 2-Acetamido-1,3-bis(tert-butyldimethylsilyloxy)-2-(2-(4-formylphenyl)ethyl)propane | HCID 15516678 | — |
| 生成物 | 2-Acetamido-1,3-bis(tert-butyldimethylsilyloxy)-2-(2-(4-(1-hydroxy-7-phenylheptyl)phenyl)ethyl)propane | HCID 22178488 | 65.2% |
反応手順
2-Acetamido-1,3-bis(tert-butyldimethylsilyloxy)-2-(2-(4-formylphenyl)ethyl)propane (3.0 g) and 1-bromo-6-phenylhexane (3.1 g) were reacted and treated in the same manner as in Working example 1(6) to give the title compound (2.6 g) as a pale yellow oily substance.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06214873B1 |
| 出典データセット | uspto-grants-2001_04 |
| ORD ID | ord-00dbabee8efe4793907689682cd0e8c0 |
| 出典メモ | uspto-grants-2001_04 |