HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → Baccatin III isopropanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Hexane | HCID 8058 | — |
| Reactant | Baccatin Iii | HCID 65366 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Baccatin III isopropanol | HCID 86756610 | — |
Reaction Steps
Baccatin III (100 mg, 0.17 mmol) was dissolved in dichloromethane (4 mL). Isopropanol was added (130 uL, 1000%), and the resulting solution was allowed to stir for 1 h. Hexane was added to the cloud point, and crystallization began. The baccatin III, 2-propanol complex (85 mg, 77%) was collected by filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06215000B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-faa71747695648ada0aeab7e1000d413 |
| Source note | uspto-grants-2001_04 |