HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Hexene → 5-Decenoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Hexene | HCID 11597 | — |
| Reactant | 5-Hexenoic Acid | HCID 15308 | — |
| Reactant | Dec-5-enyl acetate | HCID 38027 | — |
| Catalyst | HCID 178479819 | HCID 178479819 | — |
| Product | 5-Decenoic acid | HCID 53400879 | — |
Reaction Steps
FIG. 6 shows an alternative synthesis of 5-decenyl acetate, in which 1-hexene is reacted with 5-hexenoic acid in the presence of Grubbs' catalyst to produce 5-decenoic acid that can be recrystallized, reduced to an alcohol, and acetylated to yield a greater than 90% E-5-decenyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06215019B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-adf99e6f273840459f17678167ea6b71 |
| Source note | uspto-grants-2001_04 |