HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyanophenol → HCID 532712, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyanophenol | HCID 13019 | — |
| Reactant | Valeryl chloride | HCID 61186 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 532712 | HCID 532712 | — |
Reaction Steps
This compound was prepared by reacting 4-hydroxybenzonitrile with valeryl chloride in the presence of triethylamine to give 4-cyanophenyl valerate which was subjected to a Fries rearrangement with aluminium chloride to give 4-hydroxy-3-valerylbenzonitrile which was reduced with sodium borohydride to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06215001B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-756e263eecda4e77835584bb6fb72301 |
| Source note | uspto-grants-2001_04 |