Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | Iridium | HCID 23924 | — |
| Reactant | Tantalum | HCID 23956 | — |
| Catalyst | Titanium | HCID 23963 | — |
| Product | HCID 178514811 | HCID 178514811 | — |
Reaction Steps
After the roughened titanium substrate surface was heat treated, it was painted with a n-butanol solution containing salts of iridium and tantalum. The ratio of iridium to tantalum in the solution was about 65% to 35% by weight. The solution was allowed to dry at ambient temperature for approximately 20 minutes. The painted titanium substrate was subsequently heat treated in a furnace having an oxygen containing atmosphere at approximately 500° C. for approximately 20-30 minutes to form an iridium oxide/tantalum oxide composite coating. The process of painting and heat treating the titanium substrate was repeated to obtain a first layer having a total loading of 2.0 g/m2. After the desired loading was achieved, the anode was heat treated for approximately one hour at approximately 500° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06217729B1 |
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| Source dataset | uspto-grants-2001_04 |
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| ORD ID | ord-c7848c10c67f4658b8f52f05a07d6b97 |
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| Source note | uspto-grants-2001_04 |
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